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Abstract Clinopyroxene is a rock-forming mineral that commonly hosts melt inclusions in mafic to intermediate composition volcanic and plutonic rocks. It is highly resistant to alteration compared to other co-existing phenocrysts such as plagioclase. Several recent studies have 40Ar/39Ar dated clinopyroxene in Neoproterozoic to Miocene basalts and dolerites. To assess the viability of the technique at the youngest end of the geologic time scale, we performed 40Ar/39Ar incremental heating experiments on clinopyroxene-hosted melt inclusions from a variety of mafic lithologies and tectonic settings. Most samples produced precise plateau ages including several Quaternary basalts to andesites as young as 0.6 Ma. All data are indistinguishable from new and/or published 40Ar/39Ar ages on groundmass or plagioclase from the same samples. The source of potassium (K) and resulting 40Ar* within clinopyroxene has been debated, but thus far has only been inferred based on 40Ar/39Ar data. Using electron probe microanalysis (EPMA) we show that there is negligible K in the clinopyroxene host, but substantial K (e.g., 1–4 wt%) in trapped melt inclusions and minor amounts in plagioclase inclusions. Thus, melt inclusions, which are common in phenocrysts in basaltic magmas, can be used to obtain accurate and precise 40Ar/39Ar ages for difficult-to-date volcanic and plutonic rocks from the Precambrian to the Pleistocene. 

Abstract The northwest-trending transition zone (TZ) in Arizona (southwestern United States) is an ~100-km-wide physiographic province that separates the relatively undeformed southwestern margin of the Colorado Plateau from the hyperextended Basin and Range province to the southwest. The TZ is widely depicted to have been a Late Cretaceous–Paleogene northeast-dipping erosional slope along which Proterozoic rocks were denuded but not significantly deformed. Our multi-method thermochronological study (biotite 40Ar/39Ar, zircon and apatite [U-Th-Sm]/He, and apatite fission track) of Proterozoic rocks in the Bradshaw Mountains of the west-central Arizona TZ reveals relatively rapid cooling (~10 °C/m.y.) from temperatures of >180 °C to <60 °C between ca. 70 and ca. 50 Ma. Given minimal ca. 70–50 Ma upper-crustal shortening in the TZ, we attribute cooling to exhumation driven by northeastward bulldozing of continental lower crust and mantle lithosphere beneath it by the Farallon flat slab. Bulldozing is consistent with contemporaneous (ca. 70–50 Ma) underplating and initial exhumation of Orocopia Schist to the southwest in western Arizona and Mesozoic garnet-clinopyroxenite xenoliths of possible Mojave batholith keel affinity in ca. 25 Ma TZ volcanic rocks. 

Abstract The Pinaleño Mountains of southeastern Arizona is the eastern‐most metamorphic core complex in the southern U.S. and northern Mexican Cordillera. This study investigates the thermal history and exhumation record of the Pinaleño core complex using mica⁴⁰Ar/³⁹Ar, apatite and zircon (U‐Th)/He, and apatite fission‐track thermochronometers. The Pinaleño Mountains experienced two periods of rapid cooling during the Cenozoic. The first period, from ca. 27 to 21 Ma, records tectonic exhumation related to the development of the core complex and extensional shear zone. This period was followed by a relatively quiescent interval from 21 to 13.5 Ma that records little to no exhumation. The second period of rapid cooling, from 13.5 to 11 Ma, records tectonic exhumation related to high‐angle normal faulting, characteristic of the Basin and Range province. The exhumation timing of the Pinaleño core complex matches previously recognized spatiotemporal trends in the southern Basin and Range province and indicates that core complex exhumation in this region started in southeastern Arizona (ca. 32–33°N) and migrated both northward and southward. These trends correlate well with the latitude and timing of subduction of the Pacific‐Farallon spreading ridge and the migration of the Mendocino (northward) and Rivera (southward) triple junctions. Spatiotemporal core complex exhumation trends also correlate well with regional magmatism associated with the mid‐Cenozoic flare‐up, including syn‐extensional intrusive rocks found in the footwalls of core complexes. 

Rhyolitic melt that fuels explosive eruptions often originates in the upper crust via extraction from crystal-rich sources, implying an evolutionary link between volcanism and residual plutonism. However, the time scales over which these systems evolve are mainly understood through erupted deposits, limiting confirmation of this connection. Exhumed plutons that preserve a record of high-silica melt segregation provide a critical subvolcanic perspective on rhyolite generation, permitting comparison between time scales of long-term assembly and transient melt extraction events. Here, U-Pb zircon petrochronology and 40 Ar/ 39 Ar thermochronology constrain silicic melt segregation and residual cumulate formation in a ~7 to 6 Ma, shallow (3 to 7 km depth) Andean pluton. Thermo-petrological simulations linked to a zircon saturation model map spatiotemporal melt flux distributions. Our findings suggest that ~50 km 3 of rhyolitic melt was extracted in ~130 ka, transient pluton assembly that indicates the thermal viability of advanced magma differentiation in the upper crust. 

Abstract The 40Ar/39Ar dating method is among the most versatile of geochronometers, having the potential to date a broad variety of K-bearing materials spanning from the time of Earth’s formation into the historical realm. Measurements using modern noble-gas mass spectrometers are now producing 40Ar/39Ar dates with analytical uncertainties of ∼0.1%, thereby providing precise time constraints for a wide range of geologic and extraterrestrial processes. Analyses of increasingly smaller subsamples have revealed age dispersion in many materials, including some minerals used as neutron fluence monitors. Accordingly, interpretive strategies are evolving to address observed dispersion in dates from a single sample. Moreover, inferring a geologically meaningful “age” from a measured “date” or set of dates is dependent on the geological problem being addressed and the salient assumptions associated with each set of data. We highlight requirements for collateral information that will better constrain the interpretation of 40Ar/39Ar data sets, including those associated with single-crystal fusion analyses, incremental heating experiments, and in situ analyses of microsampled domains. To ensure the utility and viability of published results, we emphasize previous recommendations for reporting 40Ar/39Ar data and the related essential metadata, with the amendment that data conform to evolving standards of being findable, accessible, interoperable, and reusable (FAIR) by both humans and computers. Our examples provide guidance for the presentation and interpretation of 40Ar/39Ar dates to maximize their interdisciplinary usage, reproducibility, and longevity.